Materials characterization

Image
Operatore in un laboratorio di fisica

For information, please send an e-mail to
Dr Luisa Raimondo
e-mail: servizi-imprese.mater@unimib.it
phone: +39 02 6448 5110
Via R. Cozzi 55, 20125 Milano
U5 Building, 2nd Floor, Room 2072

 

Thermoluminescence authentication
Cost per measurement: 225.00 €

Thermoluminescence dating
Cost per measurement: 1100.00 €

Optically Stimulated Emission dating
Cost per measurementi: 860.00 €

Radiocarbon dating
Cost per measurement:  480.00 €

Dendrochronology (dating)
Cost per measurement: 156.00 €

Elemental analysis (C, H, N, S)
Cost per measurement: 38.50 €

Rehydroxylation dating
Cost per measurement: 1100.00 €

Gravimetric Analysis for the determination of water content
Cost per measurement: 852.00 €

Elemental analysis (C, H, N, S)
Equipment: Elementar MicroCUBE
Cost per measurement: 38.50 €

Gravimetric Analysis for the determination of water content
Equipment: Quantachrome Instruments Aquadyne DVS2
Cost per measurement: 852.00 €

Thermogravimetric Analysis (TGA)
Equipment: TGA/DSC1 STARe SYSTEM (Mettler Toledo)
Cost per sample: 132.00 €

Thermogravimetric Analysis coupled to Infrared Spectroscopy (TGA/FTIR). Determination of the composition of the gaseous reaction products
Equipment: TGA/DSC1 STARe SYSTEM (Mettler Toledo)
Cost per sample: 198.00 €

Non-invasive EDXRF Analysis
Equipment: Artax (Bruker)
Cost per sample: 200.00 €

DSC for polymer analysis (3 runs)
Equipment: DSC1 (Mettler Toledo)
Cost per measurement: 160.00 €

GC-MS analysis (within 2000 u.m.a. electron impact ionization)
Equipment: Clarus 600 (Perkin-Elmer)
Cost per hour: 125.00 €

Electron Spin Resonance
Equipment: Bruker EMX 10/12
Cost per sample: 209.00 €

Laser Ablation ICP Mass Spectrometre
Equipment: Elan DRC II (Perkin Elmer)
Half day cost: 506.00 €

FTIR Spectroscopy
Equipment: FT/IR-6200 (Jasco, Jasco Corporation)
Cost per sample: 141.50 €

FTIR Spectroscopy at low temperature
Equipment: FT/IR-6200 (Jasco, Jasco Corporation)
Cost per sample: 201.00 €

MICRO-FTIR Spectroscopy
Equipment: Nicolet-iN10 (ThermoScientific)
Half day cost (technical assistance included): 279.00 €

FTIR-ATR Spectroscopy (liquid and solid samples)
Equipment: Spectrum 100 (Perkin Elmer)
Cost per hour: 148.00 €

FTIR-ATR Spectroscopy (liquid and solid samples)
Equipment: 
Cost per hour: 148.00 €

NMR Spectroscopy in liquid solution
Equipment: AVANCE NEO 400MHz (Bruker)
Cost per hour: 192.00 €

Solid State NMR Spectroscopy
Equipment: Avance 300 (Bruker)
Cost per hour: 280.50 €

Time-Domain NMR analysis (TD-NMR). a) Determination of the proton content, b) determination of the rigid fraction in polymers (evaluation of the crystallinity). Single temperature experiment
Equipment: Minispec mq20 (Bruker)
Cost per measurement: 50.00 €

Time-Domain NMR analysis (TD-NMR). Determination of the relaxation time T2 or T1 for the study of the crosslink density and homogeneity in elastomers. Single temperature experiment
Equipment: Minispec mq20 (Bruker)
Cost per measurement: 90.00 €

Time-Domain NMR analysis (TD-NMR). Multiple Quantum Coherence Measurement for the study of crosslink density and homogeneity in elastomers. Single temperature experiment
Equipment: Minispec mq20 (Bruker)
Cost per measurement: 200.00 €

Gel Permeation Chromatography for the determination of polymer molecular weight
Equipment: Waters 1515 isocratic HPLC pump; Waters 2414 refractive index detector
Cost per sample: 100.00 €

EPR and EDMR measurements. X and Q band. Variable temperature (10 K ÷ 500 K)
Cost per hour: 424.00 €

Electron Spin Resonance
Equipment: Bruker EMX 10/12
Cost per sample: 209.00 €

NMR Spectroscopy in liquid solution
Equipment: AVANCE NEO 400MHz (Bruker)
Cost per hour: 192.00 €

Solid State NMR Spectroscopy
Equipment: Avance 300 (Bruker)
Cost per hour: 280.50 €

Time-Domain NMR analysis (TD-NMR). a) Determination of the proton content, b) determination of the rigid fraction in polymers (evaluation of the crystallinity). Single temperature experiment
Equipment: Minispec mq20 (Bruker)
Cost per measurement: 50.00 €

Time-Domain NMR analysis (TD-NMR). Determination of the relaxation time T2 or T1 for the study of the crosslink density and homogeneity in elastomers. Single temperature experiment
Equipment: Minispec mq20 (Bruker)
Cost per measurement: 90.00 €

Time-Domain NMR analysis (TD-NMR). Multiple Quantum Coherence Measurement for the study of crosslink density and homogeneity in elastomers. Single temperature experiment
Equipment: Minispec mq20 (Bruker)
Cost per measurement: 200.00 €

Caratteristiche I-V di celle solari
Equipment: Home made
Cost per sample: 223.00 €

Caratterizzazione I/V (corrente, voltaggio, potenza massima, efficienza totale)
Equipment: Abet Technologies - Keithley instruments
Cost per hour: 246.00 €

Misure C-V a Temperatura Ambiente ed a singola frequenza
Cost per hour: 127.00 €

Misure C-V a  Temperatura Variabile (10-500 K) ed a singola frequenza
Cost per hour: 270.00 €

Light Beam Induced Current measurments (LBIC)
Equipment: home made
Cost per sample: 228.50 €

Misura di resistività e mobilità
Equipment: home made
Cost per sample: 102.00 €

Misura di resistività e mobilità a bassa temperatura
Equipment: home made
Cost per sample: 202.00 €

Misura di tempo di vita dei portatori di carica con tecnica di Quantum Steady State PhotoConductivity Decay (QSSPCD)
Equipment: WCT-100 (Sinton Consulting)
Cost per sample: 182.00 €

Spettroscopia di impedenza
Equipment: HP 4284A (Hewlett Packard)
Half day cost: 103.50 €

Spettroscopia di impedenza elettrochimica (EIS) (1 cella)
Equipment: EG&G PARSTAT2263
Cost per sample: 114.00 €

Dynamic Mechanical Analysis (DMA) of plastics and elastomers: single frequency analysis, determination of storage modulus, loss modulus and tan(delta)
Cost per sample: 300.00 €

Mechanical measurements of plastics and elastomers by means of Zwick dynamometer in traction or compression: determination of the elastic modulus, load at break, deformation at break. Minimum five specimens
Cost per analysis: 250.00 €

Optical Microscopy Imaging (transmission or reflection configuration)
Equipment: BX51 (Olympus)
Cost per hour: 115.50 €

Hot-Stage Optical Microscopy Imaging (transmission or reflection configuration). Temperature: -190°C ÷ 600°C
Equipment: BX51 (Olympus)
Cost per hour: 148.50 €

Atomic Force Microscopy (AFM) - μm-resolution images. Scans on two different regions and on two areas per region, with size between 3×3 and 100×100 μm2
Equipment: Nanoscope V Multimode AFM (Veeco)
Cost per sample: 330.00 €

Atomic Force Microscopy (AFM) - nm-resolution images. Scans on one single region
Equipment: Nanoscope V Multimode AFM (Veeco)
Cost per sample: 440.00 €

For Scanning Electron Microscopy (SEM), please contact servizi-imprese.mater@unimib.it.

Non-invasive EDXRF Analysis
Equipment: Artax (Bruker)
Cost per sample: 200.00 €

IR Photoluminescence
Equipment: home made
Cost per sample: 277.00 €

IR Photoluminescence at low temperature
Equipment: home made
Cost per hour: 323.00 €

UV-VIS Photoluminescence
Equipment: Fluorolog 3.21 (Jobin Yvon)
Cost per sample: 277.00 €

UV-VIS Photoluminescence at low temperature
Equipment: Fluorolog 3.21 (Jobin Yvon)
Cost per hour: 323.00 €

X-ray induced luminescence
Equipment: home made
(cost per day with assistance by personnel): 330.00 €

UV/vis/IR Microluminescence
Equipment: home made
Cost per sample: 275.00 €

Triple Micro-Raman Spectroscopy
Equipment: Jobin Yvon T64000
Cost per 0.5 day (technical assistance included): 266.00 €

Triple Micro-Raman Spectroscopy, deep-UV excitation
Equipment: Jobin Yvon T64000
Cost per 0.5 day (technical assistance included): 462.00 €

External Quantum Efficiency measurements (EQE or IPCE). Spectral response
Equipment: SPEQUEST (Rera systems)
Cost per hour: 284.50 €

Internal Quantum Efficiency measurements. (IQE or APCE). Spectral response.
Equipment: SPEQUEST (Rera systems)
Cost per hour: 295.50 €

Spectroscopic ellipsometry measurements on isotropic samples - thickness and refractive index in a spectral range selected between 190 and 1700 nm
Equipment: VASE (J.A. Woollam Co.)
Cost per sample: 1800.00 €

Spectroscopic ellipsometry measurements on isotropic samples - thickness and refractive index in a spectral range selected between 190 and 1700 nm, obtained using a model optimized for a first sample (applicable on samples out of a series).
Equipment: VASE (J.A. Woollam Co.)
Cost per sample: 250.00 €

Refractometry
Equipment: METRICON 2010 (Metricon Corporation)
Half day cost (technical assistance included): 253.00 €

Absorption spectrum of dye sensitized TiO2 photoanodes (5 DSC Cells - 1 dye)
Cost: 421.50 €

Absorption spectrum of dye sensitized TiO2 photoanodes (15 DSC Cells - 3 dyes)
Cost: 941.50 €

UV-vis-NIR transmission spectroscopy
Equipment: Lambda 1050+ (Perkin-Elmer)
Cost per sample (n samples ≤5): 176.00 €

UV-vis-NIR transmission spectroscopy
Equipment: Lambda 1050+ (Perkin-Elmer)
Cost per sample (n samples >5): 137.50 €

UV-vis-NIR near-normal incidence reflectance spectroscopy
Equipment: Lambda 150+ (Perkin-Elmer)
Cost per sample (n samples ≤5): 264.00 €

UV-vis-NIR near-normal incidence reflectance spectroscopy
Equipment: Lambda 1050+ (Perkin-Elmer)
Cost per sample (n samples >5): 198.00 € 

FTIR Spectroscopy
Equipment: FT/IR-6200 (Jasco, Jasco Corporation)
Cost per sample: 141.50 €

FTIR Spectroscopy at low temperature
Equipment: FT/IR-6200 (Jasco, Jasco Corporation)
Cost per sample: 201.00 €

FTIR-ATR Spectroscopy (liquid and solid samples)
Equipment: Spectrum 100 (Perkin Elmer)
Cost per hour: 148.00 €

MICRO-FTIR Spectroscopy
Equipment: Nicolet-iN10 (ThermoScientific)
Half day cost (technical assistance included): 279.00 €

MICRO-RAMAN Spectroscopy
Equipment: Labram (Dilor – JobinYvon)
Half day cost (technical assistance included): 266.00 €

UV-VIS-NIR Spectroscopy coupled to Integrating Sphere
Equipment: Lambda 950 (Perkin-Elmer)
Half day cost: 253.00 €

Wavelength resolved thermoluminescence
Equipment: home made
Cost per day with assistance by personne): 330.00 €

For information, please contact servizi-imprese.mater@unimib.it

Static contact angle measurement (from 1 to 10 samples)
Cost per sample: 70.00 €

Static contact angle measurement (11th sample and up)
Cost per sample: 60.00 €

Advancing and receding contact angle measurement (11th sample and up)
Cost per hour: 150.00 €

Advancing and receding contact angle measurement (11th sample and up)
Cost per hour: 130.00 €

Testing with high-speed camera (1 day, with operator)
Costo a giornata: 1500.00 €

TiO2 Coating 10x10 cm2
Equipment: AUREL Mod. 900T
Cost: 541.00 €

TiO2 Coating 10x10 cm2 (custom made image)
Equipment: AUREL Mod. 900T
Cost: 1108.00 €

Thin Film Deposition (max 5x5 cm2)
Cost per deposition: 213.00 €

Fabrication of DSC cells < 0.20 cm2 for component evaluation (1 dye + 1 electrolyte) (10 DSC cells)
Cost: 860.00 €

Fabrication of DSC cells < 0.20 cm2 for component evaluation (1 dye + 5 electrolytes) (25 DSC cells)
Cost: 1370.00 €

DSC Logo - custom made image (12 logos - 5x5 cm2)
Cost: 2606.00 €

Laser cutting
Equipment: Blitz 10p (Deles)
Cost per sample: 246.00 €